tga66 - An Overview
tga66 - An Overview
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以下因為這次忘記拍照，先用一些示意圖，等之後修理其他支的機會，再來補照片
On the other hand, the secure multilayer carbonaceous chars (Figure five) manufactured within the reaction in between HCNP plus the decomposition products of PA66 can insulate the fundamental substrate from your heat source and decelerate the two the heat and mass transfer [twenty five]. As a result, it may be summarized that HCNP can proficiently Enhance the flame retardancy of PA66 subsequent the gasoline-section flame retardant mechanism.
The microtopography of HCNP is demonstrated in Figure 2. The SEM and TEM outcomes Evidently showed that the HCNP provides a spherical structure, as well as the diameter in the HCNP microsphere is about two um that has a sleek surface area.
Recently, polyphosphazene derivatives are already tested for being by far the most possible flame retardants owing for their designability and char development. For instance, novel cross-connected polyphosphazene microspheres had been synthesized with 4,four′-dihydroxy biphenyl and tannic acid as co-monomers and decorated with layered double hydroxide to Increase the flame retardancy in the epoxy resin. The outcome uncovered the EP made up of 4.0 wt% microspheres exhibited the best LOI of 29.
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Regarding the TGA final results of FR-PA66, the Tmax1 gradually shifted to the lower temperature than that on the neat PA66 with raising HCNP as a result of lower Ti of pure HCNP. Figure 1c demonstrates the Ti of HCNP is 352 °C due to the P-N bond precedence breakage amongst HCCP and DABA less than reduced temperatures. It is fascinating to check out the P-containing alkanes of FR-PA66 are detected from the TG-IR exam under four hundred °C, that's significantly distinct with the thermal decomposition merchandise of pure PA66 [twenty]. Additionally, the R-P· radicals produced by HCNP can catalyze and accelerate the breaking of C-N bonds for the α position on the PA66 molecular chain, resulting in the development of unstable amino radicals and carbonyl radicals, resulting in the decomposition in the FR-PA66.